Three-dimensional simulation of ultrasound propagation through trabecular bone structures measured by synchrotron microtomography Bossy, E., F. Padilla, F. Peyrin, and P. Laugier Physics in Medicine and Biology 50, no. 23, 5545-5556 (2005)
Résumé: Three-dimensional numerical simulations of ultrasound transmission were performed through 31 trabecular bone samples measured by synchrotron microtomography. The synchrotron microtomography provided high resolution 3D mappings of bone structures, which were used as the input geometry in the simulation software developed in our laboratory. While absorption (i.e. the absorption of ultrasound through dissipative mechanisms) was not taken into account in the algorithm, the simulations reproduced major phenomena observed in real through-transmission experiments in trabecular bone. The simulated attenuation (i.e. the decrease of the transmitted ultrasonic energy) varies linearly with frequency in the MHz frequency range. Both the speed of sound (SOS) and the slope of the normalized frequency-dependent attenuation (nBUA) increase with the bone volume fraction. Twenty-five out of the thirty-one samples exhibited negative velocity dispersion. One sample was rotated to align the main orientation of the trabecular structure with the direction of ultrasonic propagation, leading to the observation of a fast and a slow wave. Coupling numerical simulation with real bone architecture therefore provides a powerful tool to investigate the physics of ultrasound propagation in trabecular structures. As an illustration, comparison between results obtained on bone modelled either as a fluid or a solid structure suggested the major role of mode conversion of the incident acoustic wave to shear waves in bone to explain the large contribution of scattering to the overall attenuation. © 2005 IOP Publishing Ltd.
Mots-clés: Algorithms; Bone; Computer simulation; Shear waves; Wave propagation; Slow waves; Synchrotron microtomography; Ultrasonic propagation; article; bone structure; dispersion; priority journal; shear flow; simulation; structure analysis; synchrotron microtomography; three dimensional imaging; tomography; trabecular bone; velocity; Algorithms; Bone and Bones; Bone Density; Computer Simulation; Humans; Image Interpretation, Computer-Assisted; Imaging, Three-Dimensional; Models, Statistical; Models, Th
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In solid localization of finger impacts using acoustic time-reversal process Ing, R. K., N. Quieffin, S. Catheline, and M. Fink Applied Physics Letters 87, no. 20, 1-3 (2005)
Résumé: Time reversal in acoustics is a very efficient solution to focus sound back to its source in a wide range of materials including reverberating media. It expresses the following properties: A wave still has the memory of its source location. The concept presented in this letter first consists in detecting the acoustic waves in solid objects generated by a slight finger knock. In a second step, the information related to the source location is extracted from a simulated time reversal experiment in the computer. Then, an action (turn on the light or a compact disk player, for example) is associated with each location. Thus, the whole system transforms solid objects into interactive interfaces. Compared to the existing acoustic techniques, it presents the great advantage of being simple and easily applicable to inhomogeneous objects whatever their shapes. The number of possible touch locations at the surface of objects is shown to be directly related to the mean wavelength of the detected acoustic wave. © 2005 American Institute of Physics.
Mots-clés: Acoustics; Computer simulation; Object recognition; Surface treatment; Acoustic time-reversal processes; Solid localization; Source location; Acoustic waves
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Laser-based ultrasonic generation and detection of zero-group velocity Lamb waves in thin plates Prada, C., O. Balogun, and T. W. Murray Applied Physics Letters 87, no. 19, 1-3 (2005)
Résumé: A novel laser-based ultrasonic technique for the inspection of thin plates and membranes is presented, in which a modulated continuous-wave laser source is used to excite narrow bandwidth Lamb waves. The dominant feature in the acoustic spectrum is a sharp resonance peak that occurs at the minimum frequency of the first-order symmetric Lamb mode, where the group velocity of the Lamb wave goes to zero while the phase velocity remains finite. Experimental results with the laser source and receiver on epicenter demonstrate that the zero-group velocity resonance generated with a low-power modulated excitation source can be detected using a Michelson interferometer coupled to a lock-in amplifier. This resonance peak is sensitive to the thickness and mechanical properties of plates and may be suitable, for example, for the measurement and mapping of nanoscale thickness variations. © 2005 American Institute of Physics.
Mots-clés: Continuous wave laser; Ultrasonic technique; Zero-group velocity; Bandwidth; Continuous wave lasers; Laser beam effects; Resonance; Thickness measurement; Velocity measurement; Ultrasonic waves
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Wave propagation through a random array of pinned dislocations: Velocity change and attenuation in a generalized Granato and Lücke theory Maurel, A., V. Pagneux, F. Barra, and F. Lund Physical Review B - Condensed Matter and Materials Physics 72, no. 17 (2005)
Résumé: A quantitative theory of the elastic wave damping and velocity change due to interaction with dislocations is presented. It provides a firm theoretical basis and a generalization of the Granato and Lücke model [J. Appl. Phys. 27, 583 (1956)]. This is done considering the interaction of transverse (T) and longitudinal (L) elastic waves with an ensemble of dislocation segments randomly placed and randomly oriented in an elastic solid. In order to characterize the coherent wave propagation using multiple scattering theory, a perturbation approach is used, which is based on a wave equation that takes into account the dislocation motion when forced by an external stress. In our calculations, the effective velocities of the coherent waves appear at first order in perturbation theory while the attenuations have a part at first order due to the internal viscosity and a part at second order due to the energy that is taken away from the incident direction. This leads to a frequency dependence law for longitudinal and transverse attenuations that is a combination of quadratic and quartic terms instead of the usual quadratic term alone. Comparison with resonant ultrasound spectroscopy (RUS) and electromagnetic acoustic resonance (EMAR) experiments is proposed. The present theory explains the difference experimentally observed between longitudinal and transverse attenuations [Ledbetter, J. Mater. Res. 10, 1352 (1995)]. © 2005 The American Physical Society.
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Time reversal of electromagnetic waves and telecommunication Lerosey, G., J. De Rosny, A. Tourin, A. Derode, G. Montaldo, and M. Fink Radio Science 40, no. 6 (2005)
Résumé: [1] Time reversal (TR) communication in various configurations (single input, single output (SISO); multiple inputs, single output (MISO); or multiple inputs, multiple outputs (MIMO)) is studied. In particular, we report an experimental demonstration of time reversal focusing with electromagnetic waves in a SISO scheme. An antenna transmits a 1 μs electromagnetic pulse at a central frequency of 2.45 GHz in a high-Q cavity. Another antenna records the strongly reverberated signal. The time-reversed wave is built and transmitted back by the same antenna acting now as a time reversal mirror. The wave is found to converge to its initial source and is compressed in time. The quality of focusing is determined by the frequency bandwidth and the spectral correlations of the field within the cavity. A spatial focusing of the compressed pulse is also shown. This experiment is the first step for a communication scheme based on time reversal. It would be very interesting for ultrawideband communication in complex media since TR would permit compensation for delay spreading. MISO and MIMO TR communications are discussed on the basis of small-scale experiments with ultrasound. In particular, the binary error rate of the method is studied as a function of both data rate and external noise. A simple theoretical approach explains the results. Copyright 2005 by the American Geophysical Union.
Mots-clés: Antennas; Bandwidth; Error analysis; Functions; Telecommunication systems; Binary error rate; Complex media; Ultrawideband communication; Electromagnetic waves
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Interaction between an elastic wave and a single pinned dislocation Maurel, A., V. Pagneux, F. Barra, and F. Lund Physical Review B - Condensed Matter and Materials Physics 72, no. 17 (2005)
Résumé: Acoustic, and more generally elastic, waves in solids are damped by several mechanisms, among which dislocation motion is believed to play an important role. This is because an elastic wave interacts with a dislocation causing it to oscillate in response, and the resulting transfer of energy from wave to dislocation damps the acoustic vibrations. Recently, improved experimental techniques as well as improved numerical methods have been able to probe in some detail this interaction, isolating the effect of a single dislocation, and at this stage the theory, in its analytic form, is not sufficiently developed to provide quantitative comparison with experimental data and computer simulations. There is thus a need for an improved theoretical study of this issue. In this paper, we consider the interaction of transverse (T) and longitudinal (L) polarized waves in a homogeneous and isotropic, three dimensional, continuum linear elastic medium interacting with a dislocation segment pinned at both ends. An elastic wave incident upon such a dislocation segment is scattered, and the resulting scattered wave is characterized by its scattering amplitudes, that account for possible T-L mode conversions. Such scattering amplitudes are explicitly calculated. As a consequence, it is possible to calculate the resulting interference patterns of incident with scattered wave, such as have been observed in recent experiments [Shilo and Zolotoyabko, Phys. Rev. Lett. 91, 115506 (2003)]. The energy loss per cycle is also calculated using the optical theorem and results are shown to be in qualitative agreement with the results of numerical experiments [Greaney, Comput. Mater. Sci. 25, 387 (2002)]. © 2005 The American Physical Society.
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Diffuse reverberant acoustic wave spectroscopy with absorbing scatterers De Rosny, J., C. Debever, S. Conti, and P. Roux Applied Physics Letters 87, no. 15, 1-3 (2005)
Résumé: Strong interest has been shown on the propagation of transient ultrasonic waves inside a high reverberating cavity filled with moving scatterers. A diffuse model theoretically justifies that the elastic cross section and the dynamic of the scatterers can be deduced from field correlations. Recently, experiments have been performed to also obtain the inelastic cross section of the scatterers. In this letter, we propose justifying this extension within the diffuse model. Experimental results obtained inside a 1.5 liter reverberant water tank at 900 kHz central working frequency with spheres made of materials of different absorption are presented. © 2005 American Institute of Physics.
Mots-clés: Acoustic wave spectroscopy; Diffuse model; Absorption; Diffusion; Spectroscopy; Ultrasonic waves
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Building three-dimensional images using a time-reversal chaotic cavity Montaldo, G., D. Palacio, M. Tanter, and M. Fink IEEE Transactions on Ultrasonics, Ferroelectrics, and Frequency Control 52, no. 9, 1489-1497 (2005)
Résumé: The design of two-dimensional (2-D) arrays for three-dimensional (3-D) ultrasonic imaging is a major challenge in medical and nondestructive applications. Thousands of transducers are typically needed for focusing and steering in a 3-D volume. In this article, we propose a different concept allowing us to obtain electronic 3-D focusing with a small number of transducers. The basic idea is to couple a small number of transducers to a chaotic reverberating cavity with one face in contact with the body of the patient. The reverberations of the ultrasonic waves inside the cavity create at each reflection virtual transducers. The cavity acts as an ultrasonic kaleidoscope multiplying the small number of transducers and creating a much larger virtual transducer array. By exploiting time-reversal processing, it is possible to use collectively all the virtual transducers to focus a pulse everywhere in a 3-D volume. The reception process is based on a nonlinear pulse-inversion technique in order to ensure a good contrast. The feasibility of this concept for the building of 3-D images was demonstrated using a prototype relying only on 31 emission transducers and a single reception transducer. © 2005 IEEE.
Mots-clés: Chaotic reverberating cavity; Non-linear pulse inversion; Three-dimensional imaging; Time-reversal chaotic cavity; Chaos theory; Nondestructive examination; Software prototyping; Three dimensional; Transducers; Ultrasonics; Ultrasonic imaging
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Photorefractive and photochromic properties of ruthenium-doped Bi 12SiO20 Ramaz, F., L. Rakitina, M. Gospodinov, and B. Briat Optical Materials 27, no. 10, 1547-1559 (2005)
Résumé: Ruthenium can easily be incorporated into Bi12SiO20 (BSO) and an unusually high (1.3 cm-1) photorefractive gain was measured in the diffusion regime with a krypton laser at 647 nm. One particular experiment demonstrated that electron and hole gratings could eventually be formed with different time constants, thus leading to a reduction of the gain. Several complementary spectroscopic techniques were used to characterise our crystals. Magnetic circular dichroism (MCD) demonstrated that Ru substitutes under several valences for Bi in the pseudo-octahedron formed by bismuth and oxygen atoms. This was confirmed by electron paramagnetic resonance detected either classically (EPR at 9 GHz) or optically (ODMR, 35 GHz). Photochromism was investigated via a series of absorption and MCD experiments on oxidized and reduced samples. Our results in the visible spectral range could be understood via a correlation with the behaviour of the Ru5+ and Ru3+ MCD features in the near-IR, under similar illuminations. The primary process with red light is the ionisation of electrons from the VB to the Ru 4+/3+ acceptor level and the subsequent capture of the left holes at the Ru5+/4+ level. Under blue light, paramagnetic Bi Si 4+ is formed via the ionisation of BiSi 3+. The charge transfer transitions of Ru5+ were assigned via additional experiments on Ru-doped lithium niobate and garnets. The build-up and decay of photochromism were investigated, three different behaviours being observed, depending upon the initial conditions. The three-valence-two-level model is not adequate to explain the bi-exponential temporal behaviour of photochromism. It is suggested that a third relatively shallow level, possibly associated to iron, plays an important role. © 2004 Elsevier B.V. All rights reserved.
Mots-clés: Bi12SiO20; Bismuth silicate; BSO; EPR; Magnetic circular dichroism; MCD; ODMR; Optical absorption; Photochromic; Photochromism; Photorefractive; Ru; Ruthenium; Sillenites; Doping (additives); Light absorption; Paramagnetic resonance; Photochromism; Photorefractive materials; Ruthenium; Silicate minerals; Silicon compounds; Bi12SiO20; Bismuth silicate; BSO; Magnetic circular dichroism; MCD; ODMR; Sillenites; Bismuth compounds
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Weak localization and time reversal of ultrasound in a rotational flow De Rosny, J., A. Tourin, A. Derode, P. Roux, and M. Fink Physical Review Letters 95, no. 7 (2005)
Résumé: A one-channel time-reversal (TR) experiment is performed inside a rough reverberating cavity in the presence of a rotational flow. The amplitude of the TR wave is plotted versus the distance between the TR channel and the initial source: when they coincide, it exhibits a "time-reversal enhancement" (TRE). With no flow, the TRE is the same as the coherent backscattering enhancement (CBE). But contrary to CBE, the TRE peak is shown to be insensitive to the breaking down of reciprocity due to the flow. This new effect of weak localization is sustained by a diagrammatic approach. © 2005 The American Physical Society.
Mots-clés: Coherent backscattering enhancement (CBE); Weak localization; Backscattering; Coherent light; Light sources; Rotational flow; Ultrasonics
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In vivo anterior segment imaging in the rat eye with high speed white light full-field optical coherence tomography Grieve, K., A. Dubois, M. Simonutti, M. Paques, J. Sahel, J.-F. Le Gargasson, and C. Boccara Optics Express 13, no. 16, 6286-6295 (2005)
Résumé: We present a new high speed full-field optical coherence tomography (OCT) instrument, the first full-field OCT system that is capable of in vivo ocular imaging. An isotropic resolution of ∼ 1 μm is achieved thanks to the use of a xenon arc lamp source and relatively high numerical aperture microscope objectives in a Linnik-type interferometer. Full-field illumination allows the capture of two-dimensional en face images in parallel, using a fast CMOS camera as detector array. Each en face image is acquired in a 4 ms period, at a maximum repetition rate of 250 Hz. Detection sensitivity per en face image is 71 dB. Higher sensitivity can be achieved by image correlation and averaging, although frame rate is reduced. We present the first preliminary results of in vivo imaging in the anterior segment of the rat eye, which reveal some cellular features in the corneal layers. © 2005 Optical Society of America.
Mots-clés: CMOS integrated circuits; Coherent light; Image analysis; Imaging techniques; Interferometers; Light sources; Sensitivity analysis; Tomography; Video cameras; Image correlation; In vivo imaging; Optical coherence tomography; Optical instruments
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Ultrahigh resolution ex vivo ocular imaging using ultrashort acquisition time en face optical coherence tomography Grieve, K., G. Moneron, A. Dubois, J.-F. Le Gargasson, and C. Boccara Journal of Optics A: Pure and Applied Optics 7, no. 8, 368-373 (2005)
Résumé: We explore the potential and the limitations of a new ultrashort acquisition time en face optical coherence tomography (OCT) technique in application to ocular imaging. The instrument is based on the Linnik interferometer, illuminated with a xenon flash lamp. Transverse resolution is determined by the numerical aperture of the microscope objectives, whilst axial resolution is governed by the source coherence length. An isotropic resolution of ∼1 νm is achieved. The acquisition speed is determined by the flash pulse duration, i.e. 10 νs. A full two-dimensional en face tomographic image is captured in this time period. Preliminary results of imaging in ex vivo ocular tissues of the rat are presented and compared with results obtained using our original full-field OCT system. The possibility of extension to in vivo imaging is discussed. © IOP Publishing Ltd.
Mots-clés: Medical and biological imaging; Medical optics instrumentation; Ophthalmology; Optical coherence tomography; Cameras; Charge coupled devices; Fiber optics; Luminescence; Medical imaging; Ophthalmology; Solid state lasers; Tissue; Xenon; Flash lamps; Medical and biological imaging; Medical optics instrumentation; Optical coherence tomography; Tomography
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Elastic wave propagation through a distribution of dislocations Maurel, A., V. Pagneux, D. Boyer, and F. Lund Materials Science and Engineering A 400-401, no. 1-2 SUPPL., 222-225 (2005)
Résumé: We study the coherent propagation of an elastic wave in a two-dimensional continuous elastic medium filled with dislocation arrays randomly distributed and oriented in space. This configuration reasonably mimics grain boundaries in polycrystals. Interest is in evaluating the plastic contributions to the multiple scattering of waves in polycrystals that may superpose to other known scattering processes, like scattering due to inhomogeneities of elastic properties among grains. Calculations are performed in a multiple scattering formalism, based on the derivation of the so-called mass operator, in the approximation of weak scattering. We find that sound attenuation increases when the frequency decreases, a trend opposite to the usual behavior, suggesting that dislocations could sensibly modify the acoustic properties of materials at low frequency. © 2005 Elsevier B.V. All rights reserved.
Mots-clés: Dislocations; Grain boundary; Multiple scattering; Polycrystal; Acoustic properties; Approximation theory; Grain boundaries; Polycrystals; Scattering; Wave propagation; Coherent propagation; Dislocations arrays; Mass operator; Sound attentuation; Elastic waves; wave propagation
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Human muscle hardness assessment during incremental isometric contraction using transient elastography Gennisson, J. L., C. Cornu, S. Catheline, M. Fink, and P. Portero Journal of Biomechanics 38, no. 7, 1543-1550 (2005)
Résumé: The aim of this study was to investigate the relationship between biceps brachii hardness using the transient elastography technique, and its activity level by quantifying the surface electromyographic signal (sEMG). Ten healthy subjects volunteered for this protocol. To assess the maximal biceps brachii myoelectric activity (sEMG-RMSm), subjects had to achieve their maximal voluntary contraction trial during an elbow flexion effort. They were then asked to perform an isometric biceps sEMG-RMS ramp trial in elbow flexion from 0% to 50% of their sEMG-RMSm in 120 s. A low-frequency pulse was sent every 5 s during all trials by an innovative shear elasticity probe previously placed over the belly of the biceps brachii allowing the calculation of a transverse shear modulus. The main results of this study were (i) the finding of a systematic linear relationship between the biceps brachii transverse shear moduli and the corresponding sEMG-RMS values. This was not the case when plotting transverse shear modulus versus the elbow flexion torque production. Therefore, the computation of a hardness index from the slope of individual transverse shear modulus-sEMG-RMS linear relationship was enabled; (ii) It was also found that the higher is the rest shear modulus, the lower is the hardness index, indicating that the transverse shear modulus change during contraction depends on its level at rest. Therefore, this non-invasive technique could be useful in the medical field to explore deep muscles which are unreachable by classical testing methods. It could also be applied for the follow-up of neuromuscular diseases inducing stiffness changes such as in Duchenne muscular dystrophy. © 2004 Published by Elsevier Ltd.
Mots-clés: Isometric contraction; Muscle hardness; Shear wave; Surface EMG; Young's modulus; Biomechanics; Disease control; Elastic moduli; Elasticity; Electromyography; Hardness; Neurology; Signal processing; Torque control; Biceps brachii; Isometric contraction; Surface electromyographic signal (sEMG); Transient elastography; Muscle; adult; article; biceps brachii muscle; controlled study; elastography; elbow flexion; electromyography; frequency analysis; hardness; human; human experiment; linear system;
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Resonant tunneling of acoustic waves through a double barrier consisting of two phononic crystals Van Der Biest, F., A. Sukhovich, A. Tourin, J. H. Page, B. A. Van Tiggelen, Z. Liu, and M. Fink Europhysics Letters 71, no. 1, 63-69 (2005)
Résumé: We present the acoustic analog of resonant tunneling through a double barrier in quantum mechanics. Pairs of identical phononic crystals, in both 2D and 3D, were assembled and separated by a uniform spacer, forming a resonant cavity. The ultrasonic transmission exhibits resonant peaks at frequencies inside the band gaps, where ultrasound tunneling through each phononic crystal occurs. On resonance, the measured group time is large and even predicted to increase exponentially with the thickness of the crystals in the absence of absorption, while off resonance very fast speeds are found. © EDP Sciences.
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Stroboscopic ultrahigh-resolution full-field optical coherence tomography Moneron, G., A. C. Boccara, and A. Dubois Optics Letters 30, no. 11, 1351-1353 (2005)
Résumé: We present a new technique that produces en face tomographic images with a 10-μS acquisition time per image. The setup consists of an interference microscope with stroboscopic illumination provided by a xenon arc flash lamp (10-μs flashes at 15 Hz). The tomographic images are obtained from two phase-opposed interferometric images recorded simultaneously by two synchronized CCD cameras. Transverse resolution better than 1.0 μm is achieved by use of high-numerical-aperture microscope objectives. The short coherence length of the source yields an axial resolution of 0.9 μm. 3×3 pixel binning leads to a detection sensitivity of 71 dB. Our system is suitable for various applications, particularly in biology for in vivo cellular-level imaging. © 2005 Optical Society of America.
Mots-clés: Coherent light; Image analysis; Imaging systems; Interferometers; Light polarization; Optical beam splitters; Optical image storage; Optical resolving power; Optical systems; Stroboscopes; Laser sources; Numerical aperture (NA); Optical coherence tomography (OCT); Optical imaging; Tomography; animal; article; cytology; equipment; equipment design; evaluation; eye; image enhancement; instrumentation; methodology; optical coherence tomography; phase contrast microscopy; signal processing; strobosc
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Time reversal of noise sources in a reverberation room Ribay, G., J. De Rosny, and M. Fink Journal of the Acoustical Society of America 117, no. 5, 2866-2872 (2005)
Résumé: Usually, time reversal is studied with pulsed emissions. Here, the properties of time reversal of the acoustic field emitted by noise sources in a reverberation room are studied numerically, theoretically, and experimentally. A time domain numerical simulation of a two-dimensional enclosure shows that the intensity of a time-reversed noise is strongly enhanced right on the initial source position. A theory based on the link that exists between time reversal of noise and the "well-known" time reversal of short pulse is developed. One infers that the focal spot size equals half a wavelength and the signal to noise ratio only depends on the number of transceivers in the time reversal mirror. This last property is characteristic of the time reversal of noise. Experimental results are obtained in a 5 × 3 × 3 m3 reverberation room. The working frequency range varies from 300 Hz to 2 kHz. The ability of the time reversal process to physically reconstruct the image of two noise sources is studied. To this end, care is given to the technique to separate two close random sources, and also to the influence of temperature fluctuations on the focusing quality. © 2005 Acoustical Society of America.
Mots-clés: Computer simulation; Image processing; Natural frequencies; Reverberation; Signal to noise ratio; Time domain analysis; Noise sources; Random sources; Time reversal mirrors; Time-reversed noise; Acoustic noise; acoustics; article; noise measurement; priority journal; simulation; technique; theoretical model; time; Acoustics; Models, Theoretical; Noise; Time Factors
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Encapsulation of magnetic and fluorescent nanoparticles in emulsion droplets Mandal, S. K., N. Lequeux, B. Rotenberg, M. Tramier, J. Fattaccioli, J. Bibette, and B. Dubertret Langmuir 21, no. 9, 4175-4179 (2005)
Résumé: Oils containing both fluorescent semiconductor and magnetic oxide nanoparticles are used to produce oil in water emulsions. This technique produces oil droplets with homogeneous fluorescence and high magnetic nanoparticle concentrations. The optical properties of the oil droplets are studied as a function of the droplet sizes for various concentrations of fluorescent and magnetic nanoparticles. For all concentrations tested, we find a linear variation of the droplet fluorescent intensity as a function of the droplet volume. For a given size and a given quantum dot (QD) concentration, the droplet fluorescence intensity drops sharply as a function of the magnetic nanoparticle concentration. We show that this decrease is due mainly to the strong absorption cross section of the magnetic nanoparticles and to a lesser extent to the dynamic and static quenching of the QD fluorescence. The role of the iron oxide nanoparticle localization in the droplet (surface versus volume) is also discussed. © 2005 American Chemical Society.
Mots-clés: Adsorption; Concentration (process); Encapsulation; Fluorescence; Magnetic field effects; Quenching; Semiconductor quantum dots; Synthesis (chemical); Biomolecules; Emulsion droplets; Magnetic oxides; Water emulsion; Nanostructured materials; ferric ion; ferric oxide; nanomaterial; oil; quantum dot; adsorption; article; chemistry; emulsion; fluorescence; fluorescence microscopy; magnetism; nanotechnology; particle size; surface property; time; Adsorption; Emulsions; Ferric Compounds; Fluorescenc
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Viscoelastic shear properties of in vivo breast lesions measured by MR elastography Sinkus, R., M. Tanter, T. Xydeas, S. Catheline, J. Bercoff, and M. Fink Magnetic Resonance Imaging 23, no. 2 SPEC. ISS., 159-165 (2005)
Résumé: Elastography is a technique to assess the viscoelastic properties of tissue by measuring an acoustic wave propagating though the object. Here, the technique is applied in the course of standard MR mammography to 15 patients with different pathologies (six breast cancer cases, six fibroadenoma cases and three mastopathy cases). Low-frequency mechanical waves are coupled longitudinally into the tissue in order to obtain sufficient wave amplitude throughout the entire breast. This leads to the presence of a substantial fraction of compressional waves, which contribute to the total displacement field. It is shown theoretically that the correct evaluation of these contributions from the compressional wave is rather difficult due to the almost incompressible nature of tissue. To overcome this problem, it is proposed to apply the curl-operator to the measured displacement field in order to completely remove contributions from the compressional wave. Results from simulations and a breast phantom demonstrate the feasibility of the technique. The in vivo results show a good separation between breast cancer and benign fibroadenoma utilizing the shear modulus. Breast cancer appears on average 2.2 (P<.001) times stiffer. All breast cancer cases showed a good delineation to the surrounding breast tissue with an average elevation of a factor of 3.3 (P<1.4×10 -6). The results as obtained for the shear viscosity do not indicate to be useful for separating benign from malignant lesions. © 2005 Elsevier Inc. All rights reserved.
Mots-clés: Breast lesion; Elastography; Viscoelasticity; amplitude modulation; benign tumor; breast cancer; breast disease; breast fibroadenoma; breast lesion; conference paper; elastography; frequency modulation; human; malignant neoplastic disease; mammography; measurement; nuclear magnetic resonance; pathology; priority journal; simulation; viscoelasticity; viscosity; Acoustics; Breast; Breast Diseases; Breast Neoplasms; Elasticity; Female; Fibroadenoma; Humans; Magnetic Resonance Imaging; Phantoms, Ima
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Characterization of subwavelength elastic cylinders with the decomposition of the time-reversal operator: Theory and experiment Minonzio, J.-G., C. Prada, D. Chambers, D. Clorennec, and M. Fink Journal of the Acoustical Society of America 117, no. 2, 789-798 (2005)
Résumé: The decomposition of the time-reversal operator provides information on the scattering medium. It has been shown [Chambers and Gautesen, J. Acoust. Soc. Am. 109, 2616-2624 (2001)] that a small spherical scatterer is in general associated with four eigenvalues and eigenvectors of the time-reversal operator. In this paper, the 2D problem of scattering by an elastic cylinder, imbedded in water, measured by a linear array of transducers is considered. In this case, the array response matrix has three nonzero singular values. Experimental results are obtained with linear arrays of transducers and for wires of different diameters smaller that the wavelength. It is shown how the singular value distribution and the singular vectors depend on the elastic velocities c L, c T, the density p of each wire, and on the density ρ 0 and velocity c 0 of the surrounding fluid. These results offer a new perspective towards solution of the inverse problem by determining more than scattering contrast using conventional array processing like that used in medical ultrasonic imaging. © 2005 Acoustical Society of America.
Mots-clés: Cylinders (shapes); Decomposition; Eigenvalues and eigenfunctions; Elasticity; Scattering; Transducers; Ultrasonic imaging; Medical ultrasonic imaging; Scattering medium; Subwavelegnth elastic cylinders; Time-reversal operator; Acoustic waves; acoustics; article; decomposition; liquid; mathematical analysis; priority journal; signal processing; transducer; ultrasound; velocity; waveform
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Imaging anisotropic and viscous properties of breast tissue by magnetic resonance-elastography Sinkus, R., M. Tanter, S. Catheline, J. Lorenzen, C. Kuhl, E. Sondermann, and M. Fink Magnetic Resonance in Medicine 53, no. 2, 372-387 (2005)
Résumé: MR-elastography is a new technique for assessing the viscoelastic properties of tissue. One current focus of elastography is the provision of new physical parameters for improving the specificity in breast cancer diagnosis. This analysis describes a technique to extend the reconstruction to anisotropic elastic properties in terms of a so-called transversely isotropic model. Viscosity is treated as being isotropic. The particular model chosen for the anisotropy is appealing because it is capable of describing elastic shear anisotropy of parallel fibers. The dependence of the reconstruction on the particular choice of Poisson's ratio is eliminated by extracting the compressional displacement contribution using the Helmholtz-Hodge decomposition. Results are presented for simulations, a polyvinyl alcohol breast phantom, excised beef muscle, and measurements in two patients with breast lesions (invasive ductal carcinoma and fibroadenoma). The results show enhanced anisotropic and viscous properties inside the lesions and an indication for preferred fiber orientation. © 2005 Wiley-Liss, Inc.
Mots-clés: Anisotropy; Breast cancer; MR-elastography; Steady-state; Viscosity; polyvinyl alcohol; anisotropy; article; breast cancer; breast fibroadenoma; cancer diagnosis; diagnostic accuracy; diagnostic procedure; elastic tissue; elastography; human; image quality; invasive carcinoma; mathematical analysis; nuclear magnetic resonance imaging; phantom; Poisson distribution; viscoelasticity; Algorithms; Anisotropy; Breast; Breast Neoplasms; Computer Simulation; Elasticity; Humans; Image Interpretation, Co
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Attribution of the absorption bands of ruthenium-doped yttrium gallium garnet crystals to Ru 3+, Ru 4+, and Ru 5+ 4d-ions by MCD Briat, B., F. Ramaz, H. B. Rjeily, and J. A. Hodges Optical Materials 27, no. 4, 691-697 (2005)
Résumé: Ruthenium-doped yttrium gallium garnet single crystals were grown from a PbO/PbF 2/B 2O 3 flux. Most samples are blue, occasionally green, orange or lemon yellow, depending upon the growth temperature and the amount of a divalent or tetravalent counterion. A spectroscopic study was carried out using several complementary techniques (optical absorption, MCD, and EPR). Low temperature MCD enabled discrimination among those absorption bands correlated to paramagnetic ions (Ru 3+ or Ru 5+) or diamagnetic Ru 4+ at the octahedral site. Ru 3+ dominates in the lemon yellow sample with a nominal Ge/Ru ratio of ≈7, whereas Ru 5+ is responsible for the orange colour in a crystal with Ca/Ru ≈7. The strongest MCD features above 2.2 eV could be rationalised in terms of oxygen-to-Ru n+ (n = 3-5) charge transfer transitions in octahedral complexes, whereas the 2 eV band of blue crystals is tentatively assigned to an intervalence transition implying Ru 4+. It is suggested that YIG films co-doped with ruthenium and a large amount of calcium or germanium might present interesting Faraday effect properties. © 2004 Published by Elsevier B.V.
Mots-clés: EPR; MCD; Optical absorption; Ruthenium; YGG; Yttrium gallium garnet; MCD; Rare earth ions; Transition metal ions; Yttrium gallium garnet (YGG); Charge transfer; Crystals; Doping (additives); Faraday effect; Garnets; Ions; Paramagnetic resonance; Ruthenium; Semiconducting gallium; Light absorption
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